Page:NIOSH Manual of Analytical Methods - 5600.pdf/17

 ORGANOPHOSPHORUS PESTICIDES: METHOD 5600, Issue 1, dated 15 August 1994 - Page 17 of 20 Table 8.

Applicable Working Range and Estimated LOD A.

F.

B.

C.

D.

E.

G. Applicable Working Range Estimated LOD Compound Sensitivity(2) (alphabetically) REL/LOD

1. Azinphos methyl 0.12 2. Chlorpyrifos 0.04 3. Diazinon 0.04 4. Dicrotophos 0.2 5. Disulfoton 0.04 6. Ethion 0.04 7. Ethoprop 0.04 8. Fenamiphos 0.14 9. Fonofos 0.04 10. Malathion 0.1 0.001 11. Methamidophos 0.6 0.005 12. Methyl parathion 0.04 13. Mevinphos 0.12 14. Monocrotophos 0.4 0.004 15. Parathion 0.04 16. Phorate 0.04

Atmospheric(1) mg/m 3

ppm (3)

0.02-0.6 0.0015-0.046 0.0012 167 0.02-0.6 0.0014-0.042 0.0004 500 0.01-0.3 0.0008-0.024 0.0004 250 0.025-0.75 0.0026-0.077 0.002 125 0.01-0.3 0.0009-0.027 0.0004 250 0.04-1.2 0.0025-0.076 0.0004 1000 0.01-0.3 0.0010-0.030 0.0004 (7) 0.01-0.3 0.0008-0.024 0.0014 71 0.01-0.3 0.0010-0.030 0.0004 250 1.0-30 0.074-2.2 10,000 0.02-0.6 0.0035-0.10 (7) 0.02-0.6 0.0019-0.056 0.0004 500 0.01-0.3 0.0011-0.033 0.0012 83 0.025-0.75 0.0027-0.082 63 0.005-0.15 0.0004-0.013 0.0004 125 0.005-0.15 0.0005-0.014 0.0004 125

Sample(4) µg/sample

Margin of Instrument(6) ng on column

(4) (4) Instrument Sample Atmospheric

ng on column µg/sample mg/m 3

2.4 to 72

1.2-36

0.06

2.4 to 72

1.2-36

0.02

1.2 to 36

0.6-18

0.02

3.0 to 90

1.5-45

0.1

1.2 to 36

0.6-18

0.02

4.8 to 144

2.4-72

0.02

1.2 to 36

0.6-18

0.02

1.2 to 36

0.6-18

0.07

1.2 to 36

0.6-18

0.02

6.-180 (5)

0.05

2.4 to 72

1.2-36

0.3

2.4 to 72

1.2-36

0.02

1.2 to 36

0.6-18

0.06

3.0 to 90

1.5-45

0.2

0.6 to 18

0.3-9

0.02

0.6 to 18

0.3-9

0.02

12. to 360 (5)

NIOSH Manual of Analytical Methods (NMAM), Fourth Edition, 8/15/94